These standards define density as “the mass of a cubic meter of the material at 25°C (77°F) in SI units,” and specific gravity as “the ratio of a given mass of material at 25°C (77°F) to the mass of an equal volume of water at the same temperature.” Many state DOTs also have state-specific test procedures, in addition to the ASTM and AASHTO standards. This blog post will explore the basics of what to know about specific gravity of asphalt, what equipment is needed and how it gets the job done with the Rice Test.
The Asphalt Rice Test is a routine test performed by asphalt producers, state departments of transportation, and testing labs. Reliable results from this test method depend on competent personnel, and selection of quality equipment can have a direct impact on test results. Choosing equipment that minimizes human input variables will increase accuracy and repeatability of this test, as well as increase lab efficiency.
How Does the Asphalt Rice Test Work?
The Rice Test compares the mass of the sample to its volume, excluding the air voids, by measuring the dry mass of the loose HMA sample either at the beginning of the test or at the end of the test, after it has been dried. The volume is calculated by dividing the mass of the water displaced by the sample by the unit weight of water.
An asphalt sample is prepared by heating it to a constant 135°C and separating into loose particles by hand. The sample is placed into a calibrated pycnometer and weighed, then water at 25°C (77°F) is added to cover the sample. A cover is placed on the pycnometer, and vacuum is applied. To obtain mass and volume, it is necessary to remove free and entrapped air from the asphalt sample immersed in water in the pycnometer. A vacuum pump quickly removes the free air, but mechanical agitation under vacuum by a Rice Shaker is required to completely remove entrapped air from the mixture. A final weight to determine volume is taken by suspending the pycnometer with sample in water or by completely filling the pycnometer with water.
What Equipment is Needed and What Does It Do?
There are different products available to get the job done in accordance with ASTM, AASHTO and any applicable state DOT standards. Some will be more time and labor-intensive, but more economical, while those that are automated can be significantly more time and labor-efficient.
To get started, a mechanical agitation device is required by AASHTO T 209 and ASTM D2041, and the Rice Shaker for Specific Gravity & Asphalt Rice Test provides consistent and automatic agitation. Two different set-up scenarios for using the Rice Shaker are shown below: the basic Asphalt Rice Test set-up which is more time-consuming and requires manual interaction from the operator, and the automated set-up using the AutoRice™ Digital Manometer/Controller System with PumpSaver™ Air-Drier that reduces operator and test time, and delivers results directly to the computer.
- Basic Equipment for the Asphalt Rice Test … In a typical set-up, the vacuum pump removes free air, while the Rice Shaker agitates the pycnometer to remove entrapped air. The Digital Absolute Pressure Manometer measures vacuum applied to the sample from the vacuum pump, and the Air/Gas Dryer with Drierite absorptive granules prevents water from entering the vacuum pump.
- Equipment for the Asphalt Rice Test with AutoRice™ Controller System … The new AutoRice™ Digital Manometer/Controller System allows precise control of vacuum pressure and time, and can be equipped to monitor vibration energy of the Rice Shaker or other mechanical agitator. Accuracy and repeatability is increased, while decreasing the need for constant attention to the procedure. The PumpSaver™ air drier protects the vacuum pump from moisture and optimizes efficiency.
In addition to the agitation device and other basic tools used with this test such as a vacuum container, thermometer, vacuum gage and bleeder valve, there are other products used with both set-up options, and some are highlighted below.
- A Pycnometer or Filter Flask which meets ASTM and AASHTO specifications is required for specific gravity determinations. Note that a Flask Adapter or Pycnometer Adapter set may also be required depending upon the model used. A thick-walled Glass Vacuum Flask can be used for weighing in air only.
- Either a vacuum pump or water aspirator is needed to effectively evacuate air from the container to a residual pressure of 4.0kPa (30mm of Hg) or less. If using an Oilless or High Vacuum Pump with Gauge, a trap must be installed to reduce the amount of water vapor that gets into the pump
- The standards require a Absolute Pressure Manometer or calibrated absolute pressure gauge to confirm that the specified pressure is applied, and the device must be able to measure residual pressure to 4.0kPA or less. A Mercury Manometer can be used in the Asphalt Rice Test; however, local regulations should be checked before using any mercury device. The Digital Absolute Pressure Manometer is mercury-free and environmentally-friendly; both manometers perform in compliance with the test standards.
- The Specific Gravity Water Tank is used for suspended weighing, and together with a Curing Tank Heater/Circulator, maintains the required constant temperature of 25°C + 1°C (77°F + 2°F). The Specific Gravity (relative density) Bench offers convenience in this process, with easy weighing of samples suspended in water. It holds the water tank, weighing cradle, balance, heater and circulator.
- A Balance which can be read to the nearest 0.1g, and has a minimum 10kg capacity. A weigh-below hook is needed, as well as a Weighing Cradle, when suspension weighing is performed.
When testing is complete, theoretical maximum specific gravity (gmm) is determined from the following:
- Mass of the dry sample in air
- Mass of container under water
- Mass of container with sample under water
For more specific details on testing for theoretical maximum or asphalt specific gravity and density, refer directly to the ASTM D2041 or AASHTO T 209 test standards. You can also learn more about the SGA-5R Rice Shaker for Specific Gravity & Asphalt Rice Test by viewing our video on YouTube.